Which Standards Apply to Moving Die Rheometer Testing?
In the process of rubber material research and development and quality control, vulcanization characteristic testing is a key step in determining the stability and consistency of product performance. The Moving Die Rheometer (MDR), as one of the most widely used vulcanization performance testing instruments today, is extensively applied in the fields of tires, seals, industrial rubber products, footwear materials, and high-performance elastomers.
However, when using a Rotorless Rheometer in practice, many users often face a core question:
Which standards should MDR testing be based on?
What are the differences between different standards?
How should one choose a testing specification that suits their laboratory or customer requirements?
I. The Role of the Rheometer Test for Rubber
Moving Die Rheometer is specifically designed to determine the rheological properties of rubber compounds during the curing process.
In the moving die rheometer, a rubber compound specimen positioned in a pressurized cavity is subjected to controlled heating. As the lower die produces sinusoidal oscillation, a torque sensor on the upper die detects the torque generated by the specimen.
II. Features of the Moving Die Rheometer
Equipped with advanced rheometer software, the moving die rheometer is specifically designed to analyze the curing characteristics of rubber compounds, including scorch time, cure time, cure rate, viscoelasticity, and cure plateau.
Scorch Time: Refers to the time experienced by the rubber compound during heating, from the start of temperature increase to the point before obvious crosslinking reactions occur and the torque begins to rise significantly. It reflects the processing safety of the compound—the longer the scorch time, the less likely premature crosslinking (scorching) will occur during processing, and the higher the processing safety.
Cure Time: Refers to the time required for the rubber compound from the start of vulcanization until the crosslinking reaction reaches a stable state (the torque reaches a maximum or stable value). It determines the actual vulcanization process duration of rubber products and is the core basis for setting production process parameters.
Cure Rate: Reflects the speed of the crosslinking reaction of the rubber compound during vulcanization, usually expressed as the reciprocal of the cure time or the slope of the torque rise stage. The cure rate directly affects production efficiency and also influences the final properties of the compound.
Viscoelasticity: The comprehensive viscous and elastic characteristics of the rubber compound during the vulcanization process, reflected through the dynamic changes in torque. Viscoelasticity directly affects the mechanical properties of rubber products (such as tensile strength, elasticity, abrasion resistance, etc.).
Cure Plateau: Refers to the stage after the rubber compound reaches a stable vulcanized state, during which the torque remains constant. The magnitude of torque during the plateau reflects the sufficiency of the crosslinking reaction. A longer plateau indicates better vulcanization stability of the compound and more stable performance of the final product.
III. Which Standards Does the MDR Rheometer Comply With?
The Moving Die Rheometer complies with the following standards:
GB/T 16584-1996, ISO 6502-3:2018, ASTM D5289-2017
1. ISO 6502-3:2018
ISO 6502-3:2018 for determining selected vulcanization characteristics of a rubber compound by means of a rotorless curemeter is one of the internationally recognized standards for rubber vulcanization performance testing, and it is particularly applicable to testing scenarios using a Moving Die Rheometer.
A test piece of rubber is placed in a heated cavity formed by two dies, one of which is oscillated at a given frequency and amplitude. This action exerts a shear strain on the test piece and a shear torque which depends on the stiffness (shear modulus) of the rubber. The torque that increases as vulcanization proceeds is measured by a torque sensor incorporated in the other die member. The torque is recorded autographically as a function of time.
The stiffness of the rubber test piece increases as vulcanization proceeds. The curve is complete when the recorded torque rises either to an equilibrium value or to a maximum value (see ISO 6502-1).
2. ASTM D5289-2017
ASTM D5289 Standard Test Method for Rubber Property—Vulcanization Using Rotorless Cure Meters.
This test method is used to determine the vulcanization characteristics of (vulcanizable) rubber compounds. It may be used for quality control in rubber manufacturing processes, for research and development testing of raw rubber compounded in an evaluation formulation, and for evaluating various raw materials used in preparing (vulcanizable) rubber compounds.
The test specimen in a rotorless cure meter approaches the test temperature in a shorter time, and there is a better temperature distribution in the test specimen due to the elimination of the unheated rotor found in oscillating disk cure meters.
Several manufacturers produce rotorless cure meters with design differences that may result in different torque responses and cure times for each design. Correlations of test results between cure meters of different designs should be established for each compound tested and for each set of test conditions.
3. GB/T 16584-1996
GB/T 16584-1996 is one of the important standards formulated in China for rubber vulcanization characteristic testing and has long been widely adopted in the domestic rubber industry. This standard specifies in detail the test methods for determining rubber vulcanization characteristics using rotorless or moving die rheometers.
The characteristics of this mdr test rubber standard include:
It is applicable to most general-purpose rubbers and formulation systems.
It clearly specifies requirements for test temperature, oscillation frequency, and strain conditions.
The Moving Die Rheometer strictly follows appropriate testing standards. Whether GB/T, ISO, or ASTM, the existence of these standards is intended to ensure reliable test data and compliant product quality, and they are also an important guarantee for promoting industry standardization and high-quality development.
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